Levalbuterol Related Compound D (30 mg) (5-[2-{(1,1-dimethylethyl)amino}-1-hydroxyethyl]-2-hydroxy-benzaldehyde sulfate)

Name	Albuterol Aldehyde
Synonyms	Albuterol Aldehyde Levalbuterol USP RC D Levalbuterol Related CoMpound D Salbutamol Impurity 4(Salbutamol EP Impurity D) 5-(2-tert-Butylamino-1-hydroxyethyl)-2-hydroxybenzaldehyde 5-[(1RS)-2-[(1,1-diMethylethyl)aMino]-1-hydroxyethyl]-2-hydroxybenzaldehyde Levalbuterol Related Compound D (30 mg) (5-[2-{(1,1-dimethylethyl)amino}-1-hydroxyethyl]-2-hydroxy-benzaldehyde sulfate)
CAS	156339-88-7
EINECS	604-604-1

HS Code

2922504500

Introduction	salbutamol impurity D is an impurity produced during the synthesis of salbutamol. Salbutamol impurity D not only retains the chemical structure of the parent nucleus of β-agonists to the greatest extent, but also introduces-CHO, which can be coupled with proteins, through chemical synthesis. The synthesis method is simple, the purity and yield were high.
Application	using salbutamol impurity D as a raw material, an antigen system suitable for animal immunization is prepared to immunize animals, the titer, specificity and Affinity of the obtained antibody are good; The obtained antibody is used in the enzyme-linked immunosorbent assay kit, which can simultaneously detect clenbuterol, salbutamol, sebuterol, tobuterol, bromobuterol, bromoclobuterol six drugs, easy to use, low cost detection.
preparation	1.0G salbutamol, dissolved in 20ml N,N-dimethylformamide, then, 10 mol% of tetramethylpiperidine oxide, 10 mol% of tetrabutylammonium chloride and 20ml of 0.5mol/L NaHCO3 aqueous solution were added, and after stirring for 30min at room temperature, add 1.1 molar equivalent of N-chlorosuccinimide, reaction at room temperature after 2~5H, remove most of the solvent, ethyl acetate extraction, washing, drying, remove the solvent column chromatography purification, A white solid salbutamol monooxide, I .e., Salbutamol impurity D, was obtained.

Last Update：2024-04-09 21:54:55

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Levalbuterol Related Compound D (30 mg) (5-[2-{(1,1-dimethylethyl)amino}-1-hydroxyethyl]-2-hydroxy-benzaldehyde sulfate) Request for Quotation